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Research Articles
Effect of different air-drying time on the microleakage of single-step self-etch adhesives
Horieh Moosavi, Maryam Forghani, Esmatsadat Managhebi
Restor Dent Endod 2013;38(2):73-78.   Published online May 28, 2013
DOI: https://doi.org/10.5395/rde.2013.38.2.73
AbstractAbstract PDFPubReaderePub
Objectives

This study evaluated the effect of three different air-drying times on microleakage of three self-etch adhesive systems.

Materials and Methods

Class I cavities were prepared for 108 extracted sound human premolars. The teeth were divided into three main groups based on three different adhesives: Opti Bond All in One (OBAO), Clearfil S3 Bond (CSB), Bond Force (BF). Each main group divided into three subgroups regarding the air-drying time: without application of air stream, following the manufacturer's instruction, for 10 sec more than manufacturer's instruction. After completion of restorations, specimens were thermocycled and then connected to a fluid filtration system to evaluate microleakage. The data were statistically analyzed using two-way ANOVA and Tukey-test (α = 0.05).

Results

The microleakage of all adhesives decreased when the air-drying time increased from 0 sec to manufacturer's instruction (p < 0.001). The microleakage of BF reached its lowest values after increasing the drying time to 10 sec more than the manufacturer's instruction (p < 0.001). Microleakage of OBAO and CSB was significantly lower compared to BF in all three drying time (p < 0.001).

Conclusions

Increasing in air-drying time of adhesive layer in one-step self-etch adhesives caused reduction of microleakage, but the amount of this reduction may be dependent on the adhesive components of self-etch adhesives.

Citations

Citations to this article as recorded by  
  • Species profile of volatile organic compounds emission and health risk assessment from typical indoor events in daycare centers
    Hailin Zheng, Júlia Csemezová, Marcel Loomans, Shalika Walker, Florent Gauvin, Wim Zeiler
    Science of The Total Environment.2024; 918: 170734.     CrossRef
  • Development of Drying Process for Removal of Residual Moisture from Biomass Pretreated with Ethanol and Its Kinetic and Thermodynamic Analysis
    Seo-Young Park, Jin-Hyun Kim
    Biotechnology and Bioprocess Engineering.2021; 26(5): 814.     CrossRef
  • Effect of 9.3 μm CO2 and 2.94 μm Er:YAG Laser vs. Bur Preparations on Marginal Adaptation in Enamel and Dentin of Mixed Class V Cavities Restored With Different Restorative Systems
    Clara Isabel Anton y Otero, Enrico Di Bella, Ivo Krejci, Tissiana Bortolotto
    Frontiers in Dental Medicine.2021;[Epub]     CrossRef
  • Development of Drying Process for Removal of Residual Solvent from Crystalline Vancomycin and Kinetic and Thermodynamic Analysis Thereof
    Tae-Hun Yoon, Jin-Hyun Kim
    Biotechnology and Bioprocess Engineering.2020; 25(5): 777.     CrossRef
  • Effect of adhesive air-drying time on bond strength to dentin: A systematic review and meta-analysis
    Mohamed M. Awad, Ali Alrahlah, Jukka P. Matinlinna, Hamdi Hosni Hamama
    International Journal of Adhesion and Adhesives.2019; 90: 154.     CrossRef
  • Optical Evaluation of Enamel Microleakage with One-Step Self-Etch Adhesives
    Alaa Turkistani, Maha Almutairi, Nouf Banakhar, Reem Rubehan, Sulafa Mugharbil, Ahmed Jamleh, Adnan Nasir, Turki Bakhsh
    Photomedicine and Laser Surgery.2018; 36(11): 589.     CrossRef
  • Improved drying method for removal of residual solvents from paclitaxel by pre-treatment with ethanol and water
    Chung-Gi Lee, Jin-Hyun Kim
    Process Biochemistry.2015; 50(6): 1031.     CrossRef
  • 1,746 View
  • 3 Download
  • 7 Crossref
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Effect of moisture and drying time on the bond strength of the one-step self-etching adhesive system
Yoon Lee, Jeong-Won Park
Restor Dent Endod 2012;37(3):155-159.   Published online August 29, 2012
DOI: https://doi.org/10.5395/rde.2012.37.3.155
AbstractAbstract PDFPubReaderePub
Objectives

To investigate the effect of dentin moisture degree and air-drying time on dentin-bond strength of two different one-step self-etching adhesive systems.

Materials and Methods

Twenty-four human third molars were used for microtensile bond strength testing of G-Bond and Clearfil S3 Bond. The dentin surface was either blot-dried or air-dried before applying these adhesive agents. After application of the adhesive agent, three different air drying times were evaluated: 1, 5, and 10 sec. Composite resin was build up to 4 mm thickness and light cured for 40 sec with 2 separate layers. Then the tooth was sectioned and trimmed to measure the microtensile bond strength using a universal testing machine. The measured bond strengths were analyzed with three-way ANOVA and regression analysis was done (p = 0.05).

Results

All three factors, materials, dentin wetness and air drying time, showed significant effect on the microtensile bond strength. Clearfil S3 Bond, dry dentin surface and 10 sec air drying time showed higher bond strength.

Conclusions

Within the limitation of this experiment, air drying time after the application of the one-step self-etching adhesive agent was the most significant factor affecting the bond strength, followed by the material difference and dentin moisture before applying the adhesive agent.

Citations

Citations to this article as recorded by  
  • An in vitro study on comparative evaluation of shear bond strength of bioactive composite to tooth structure with various dentin conditioning agents
    Priyanka Pokkula, Shaik Mohammed Asif, Abdullah Alqarni, Shahabe Saquib Abullais, Shaik Mohamed Shamsudeen, Syed M Yassin, Abosofyan S. Atta, Wahaj Ahmad Khan
    AIP Advances.2025;[Epub]     CrossRef
  • The Influence of Drying Time, Application Mode, and Agitation on the Dentin Bond Strength of a Novel Mesoporous Bioactive Glass-Containing Universal Dentin Adhesive
    Jiyoung Kwon, Jungwon Kim, Dongseok Choi, Duck-Su Kim
    Journal of Functional Biomaterials.2025; 16(7): 247.     CrossRef
  • The occluding effects of layered calcium phosphate and cyanoacrylate on dentinal tubules: a SEM study
    Özge Uzuner Bilgiç, Sühan Gürbüz, Altan Dogan
    BMC Oral Health.2025;[Epub]     CrossRef
  • Shear bond strengths of two newly marketed self‐adhesive resin cements to different substrates: A light and scanning electron microscopy evaluation
    Cansu Atalay, Uzay Koc Vural, Ivana Miletic, Sevil Gurgan
    Microscopy Research and Technique.2022; 85(5): 1694.     CrossRef
  • The effect of curing mode of dual-cure resin cements on bonding performance of universal adhesives to enamel, dentin and various restorative materials
    Erick LUZ MADRIGAL, Antonin TICHY, Keiichi HOSAKA, Masaomi IKEDA, Masatoshi NAKAJIMA, Junji TAGAMI
    Dental Materials Journal.2021; 40(2): 446.     CrossRef
  • Effect of adhesive air-drying time on bond strength to dentin: A systematic review and meta-analysis
    Mohamed M. Awad, Ali Alrahlah, Jukka P. Matinlinna, Hamdi Hosni Hamama
    International Journal of Adhesion and Adhesives.2019; 90: 154.     CrossRef
  • Effect of pre-curing of two universal adhesives on the shear bond strength of resin cement to zirconia
    Ga-Eun Son, Tae-Yub Kwon, Young Kyung Kim
    Korean Journal of Dental Materials.2019; 46(1): 21.     CrossRef
  • Bonding effectiveness of different dentin conditions on etch-and-rinse mode of two universal adhesives: the confocal laser scanning and shear bond strength
    Jounghyun Lee, Ka-Young Cho, Jin-Young Kim, Sungho Park, Byoung-Duck Roh, Yooseok shin
    Journal of Adhesion Science and Technology.2017; 31(9): 933.     CrossRef
  • Effect of dentin dehydration and composite resin polymerization mode on bond strength of two self-etch adhesives
    Pooran Samimi, Mehdi Alizadeh, Farinaz Shirban, Amin Davoodi, Maryam Khoroushi
    Contemporary Clinical Dentistry.2016; 7(1): 16.     CrossRef
  • Effect of different air-drying time on the microleakage of single-step self-etch adhesives
    Horieh Moosavi, Maryam Forghani, Esmatsadat Managhebi
    Restorative Dentistry & Endodontics.2013; 38(2): 73.     CrossRef
  • 1,369 View
  • 7 Download
  • 10 Crossref
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Original Article
Effect of a rewetting agent on dentin adhesion
Young-Gon Cho, Yil-Yoon Park, Young-Gon Lee
J Korean Acad Conserv Dent 2003;28(1):11-22.   Published online January 31, 2003
DOI: https://doi.org/10.5395/JKACD.2003.28.1.011
AbstractAbstract PDFPubReaderePub

This study compared the dentin adhesion to composite resin according to air-dry, blot dry, application of rewetting agent on air-dry or blot dry dentin surface by microleakag test and SEM observation.

For microleakage test, class V cavity preparations with dentinal margins were prepared on both buccal and lingual surfaces of 40 extracted human molars. For SEM observation, occlusal dentin of 20 extracted human molars were exposed.

After etched the dentin, prepared teeth were randomly divided into four groups;

D group: air dry for 10-15 sec., B group: blot dry with moist cotton pellet, D-R group: air dry and rewet with Aqua-Prep F for 20 sec., B-R group: blot dry and rewet with Aqua-Prep F for 20 sec.

Treated cavities and surfaces were filled or constructed using One-Step adhesives and Aelitefil composite resins. Specimens were stored in distilled water for 24 hours. For microleakage test, the specimens were thermocycled and soaked into 2% methylene blue. The specimens were sectioned longitudinally and evaluated for microleakage under steromicroscope. The data were statistically analysed by Kruskal-Wallis Test, Mann-Whitney and Wilcoxon signed ranked tests. For SEM observation, the specimens were bisectioned mesiodiatally. After decalcified and deproteinized, specimens were observed under SEM.

The results of this study were as follows;

1. The microleakges on dentinal margin were the highest in D group compared with B group, D-R group, and B-R group(p<0.05). But there was no significant difference between B group, D-R group and B-R group.

2. D group showed gap and a few resin tags between dentin and composite resin.

3. B group, D-R group, and B-R groups showed close adaptation between dentin and composite resin. It showed that resin rags in B group were numerous and long, in D-R group were few and short, in B-R group were numerous and short or long.

4. Adhesive layer showed in D-R group (10 µm) and B-R group (3 µm)

In conclusion, use of rewetting agent to dry dentin was efficient to dentin adhesion, also it did not provide reverse effect on blot dry dentin.

Citations

Citations to this article as recorded by  
  • Effect of rewetting agent on dentinal microtensile bond strength
    Hee-Young Kang, Young-Gon Cho, Jong-Uk Kim, Byung-Cheul Park, Sang-Hoon Yoo, Cheul-Hee Jin, Hee-Young Choi, Young-Jae Ki
    Journal of Korean Academy of Conservative Dentistry.2004; 29(2): 153.     CrossRef
  • 1,003 View
  • 3 Download
  • 1 Crossref
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