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  • Research Article
    Influence of 10-MDP concentration on the adhesion and physical properties of self-adhesive resin cements
    Kazuhiko Shibuya, Naoko Ohara, Serina Ono, Kumiko Matsuzaki, Masahiro Yoshiyama
    Restor Dent Endod 2019;44(4):e45.   Published online November 12, 2019
    DOI: https://doi.org/10.5395/rde.2019.44.e45
    AbstractAbstract PDFPubReaderePub
    Objectives

    Self-adhesive resin cements contain functional monomers that enable them to adhere to the tooth structure without a separate adhesive or etchant. One of the most stable functional monomers used for chemical bonding to calcium in hydroxyapatite is 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP). The aim of this study was to evaluate the influence of the10-MDP concentration on the bond strength and physical properties of self-adhesive resin cements.

    Materials and Methods

    We used experimental resin cements containing 3 different concentrations of 10-MDP: 3.3 wt% (RC1), 6.6 wt% (RC2), or 9.9 wt% (RC3). The micro-tensile bond strength of each resin cement to dentin and a hybrid resin block (Estenia C&B, Kuraray Noritake Dental) was measured, and the fractured surface morphology was analyzed. Further, the flexural strength of the resin cements was measured using the three-point bending test. The water sorption and solubility of the cements following 30 days of immersion in water were measured.

    Results

    The bond strength of RC2 was significantly higher than that of RC1. There was no significant difference between the bond strength of RC2 and that of RC3. The water sorption of RC3 was higher than that of any other cement. There were no significant differences in the three-point bending strength or water solubility among all three types of cements.

    Conclusions

    Within the limitations of this study, it is suggested that 6.6 wt% 10-MDP showed superior properties than 3.3 wt% or 9.9 wt% 10-MDP in self-adhesive resin cement.

    Citations

    Citations to this article as recorded by  
    • Comparative Evaluation of Color Stability in Bioactive and Conventional Resin Cements Under Thermal Stress Conditions
      Alaa Turkistani, Hanin E. Yeslam
      Biomimetics.2025; 10(7): 432.     CrossRef
    • A thorough assessment of 10-MDP primers in modern dental adhesive systems
      Ahmed A Abduljawad, Harraa SM Salih, Omar F Tawfiq
      Journal of Baghdad College of Dentistry.2024; 36(3): 79.     CrossRef
    • Material properties and finite element analysis of adhesive cements used for zirconia crowns on dental implants
      Megha Satpathy, Hai Pham, Shreya Shah
      Computer Methods in Biomechanics and Biomedical Engineering.2024; : 1.     CrossRef
    • Clinical reliability of self-adhesive luting resins compared to other adhesive procedures: A systematic review and meta-analysis
      Mohammed Ahmed Alghauli, Ahmed Yaseen Alqutaibi, Sebastian Wille, Matthias Kern
      Journal of Dentistry.2023; 129: 104394.     CrossRef
    • Influence of autoclave sterilization on bond strength between zirconia frameworks and Ti-base abutments using different resin cements
      Reinhold Lang, Karl-Anton Hiller, Lena Kienböck, Katrin Friedl, Karl-Heinz Friedl
      The Journal of Prosthetic Dentistry.2022; 127(4): 617.e1.     CrossRef
    • Varying 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) level improves polymerisation kinetics and flexural strength in self-adhesive, remineralising composites
      António H.S. Delgado, Nazanin Owji, Paul Ashley, Anne M. Young
      Dental Materials.2021; 37(9): 1366.     CrossRef
    • Investigating a Commercial Functional Adhesive with 12-MDPB and Reactive Filler to Strengthen the Adhesive Interface in Eroded Dentin
      Madalena Belmar da Costa, António HS Delgado, Tomás Amorim Afonso, Luís Proença, Ana Sofia Ramos, Ana Mano Azul
      Polymers.2021; 13(20): 3562.     CrossRef
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