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  • Research Articles
    Physical-mechanical, chemical and biological properties of graphene-reinforced glass ionomer cements
    Tatiane Ramos dos Santos Jordão, Laura Soares Viana Fernandes, Karla Lorene de França Leite, Adílis Alexandria, Emmanuel João Nogueira Leal Silva, Lucianne Cople Maia, Tatiana Kelly da Silva Fidalgo
    Restor Dent Endod 2024;49(4):e37.   Published online October 10, 2024
    DOI: https://doi.org/10.5395/rde.2024.49.e37
    AbstractAbstract PDFPubReaderePub
    Objectives

    This study aimed to evaluate the physical-mechanical, chemical, and biological properties of graphene-reinforced glass ionomer cements (GICs).

    Materials and Methods

    Different proportions of graphene powder were incorporated into 2 high-viscosity self-curing GIC, Ketac Molar (GKetac) and Fuji IX (GFuji), in 4 different concentrations: 0.5%, 1%, 2%, and 5%. The control groups included the GICs without graphene. Experiments were performed to analyze linear (Ra) and volumetric roughness (Sa), antimicrobial activity, radiopacity, fluoride release, microhardness, solubility, and water sorption. Data were analyzed using Kruskal-Wallis, Mann-Whitney, Wilcoxon, analysis of variance, and Tukey’s test (p ≤ 0.05).

    Results

    The GKetac 0% and GFuji0% groups presented higher Ra (4.05 and 2.72) and Sa (4.76 and 5.16), respectively. No inhibition zone was observed, and the incorporation of graphene reduced radiopacity. Moreover, there was no influence on the solubility and water sorption after 21 days. A greater fluoride release was observed in the period of 7 days for most of the groups. After 21 days, GKetac 5%, 2%, and 1% presented higher releasing than 0% and 0.5% (p ≤ 0.05).

    Conclusions

    The graphene incorporation improved the microhardness of GICs in lower concentrations. Graphene incorporation to GICs modified some physical-mechanical, and chemical, but not affected biological properties.

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    Influence of autoclave sterilization procedures on the cyclic fatigue resistance of heat-treated nickel-titanium instruments: a systematic review
    Emmanuel João Nogueira Leal Silva, Mayara Zanon, Fernanda Hecksher, Felipe Gonçalves Belladonna, Rafaela Andrade de Vasconcelos, Tatiana Kelly da Silva Fidalgo
    Restor Dent Endod 2020;45(2):e25.   Published online March 31, 2020
    DOI: https://doi.org/10.5395/rde.2020.45.e25
    AbstractAbstract PDFPubReaderePub
    Objectives

    This systematic review evaluated the influence of autoclave sterilization procedures on the cyclic fatigue resistance of heat-treated nickel-titanium (NiTi) instruments.

    Materials and Methods

    A systematic search without restrictions was conducted in the following electronic databases: PubMed, Scopus, Web of Science, ScienceDirect, Cochrane, and Open Grey. The hand search was also performed in the main endodontic journals. The eligible studies were submitted to the methodological assessment and data extraction.

    Results

    From 203 abstracts, a total of 10 articles matched the eligible criteria. After reading the full articles, 2 were excluded because of the absence of the heat-treated instruments in the experimental design and 3 due to the lack of a control group using heat-treated instruments without autoclave sterilization. From the 5 included studies, 1 presented a low risk of bias, 3 presented moderate and 1 high risk. It was observed heterogeneous findings in the included studies, with autoclave sterilization cycles increasing, decreasing or not affecting the cyclic fatigue life of heat-treated NiTi instruments. However, the retrieved studies evaluating the cyclic fatigue resistance of endodontic instruments presented different protocols and assessing outcomes, this variability makes the findings less comparable within and also between groups and preclude the establishment of an unbiased scientific evidence base.

    Conclusions

    Considering the little scientific evidence and considerable risk of bias, it is still possible to conclude that autoclave sterilization procedures appear to influence the cyclic fatigue resistance of heat-treated NiTi instruments.

    Citations

    Citations to this article as recorded by  
    • Impact of Repeated Use on Cyclic and Torsional Fatigue of 3 Rotary Files: Implications for Clinical Safety
      Raimundo Sales de Oliveira Neto, Rafael da Rocha Tavares Duarte, Marco Antonio Hungaro Duarte, Guilherme Ferreira da Silva, Murilo Priori Alcalde, Leonardo Rigoldi Bonjardim
      Journal of Endodontics.2025; 51(7): 954.     CrossRef
    • Effect of simulated clinical use and sterilization on the cyclic fatigue resistance of nickel titanium files
      Mohammad Alajemi, Ammar AbuMostafa
      PeerJ.2024; 12: e17418.     CrossRef
    • Cyclic Fatigue of Different Ni-Ti Endodontic Rotary File Alloys: A Comprehensive Review
      Dina Abdellatif, Alfredo Iandolo, Michela Scorziello, Giuseppe Sangiovanni, Massimo Pisano
      Bioengineering.2024; 11(5): 499.     CrossRef
    • Cyclic Fatigue Resistance of Rotary versus Reciprocating Endodontic Files: A Systematic Review and Meta-Analysis
      Ana De Pedro-Muñoz, Cristina Rico-Romano, Patricia Sánchez-Llobet, José María Montiel-Company, Jesús Mena-Álvarez
      Journal of Clinical Medicine.2024; 13(3): 882.     CrossRef
    • Influence of sodium hypochlorite on cyclic fatigue resistance of nickel–titanium instruments: A systematic review and meta-analysis of in vitro studies
      Alexandre Henrique dos Reis-Prado, Lucas Guimarães Abreu, Lara Cancella de Arantes, Kiani dos Santos de Paula, Sabrina de Castro Oliveira, Juliana Goto, Ana Cecília Diniz Viana, Francine Benetti
      Clinical Oral Investigations.2023; 27(11): 6291.     CrossRef
    • Cyclic fatigue resistance of EdgeTaper Platinum, Protaper Gold, and TruNatomy Prime rotary files before and after autoclave sterilization
      Rahaf A. Almohareb, Reem M. Barakat, Fahda N. Algahtani, Manal F. Alkadi
      PeerJ.2023; 11: e14656.     CrossRef
    • Effect of calcium hydroxide on fracture resistance and microhardness of dentin in human teeth
      Simar Sethi, Alpa Gupta, Ansy Hanna Kurian, Dax Abraham, Parul Chauhan, Kritika Aneja, Sucheta Jala, Arundeep Singh
      Endodontology.2022; 34(4): 223.     CrossRef
    • Effect of body temperature on the cyclic fatigue resistance of the nickel”titanium endodontic instruments: A systematic review and meta-analysis of in vitro studies
      Selventhra Savitha, Sidhartha Sharma, Vijay Kumar, Amrita Chawla, Perumal Vanamail, Ajay Logani
      Journal of Conservative Dentistry.2022; 25(4): 338.     CrossRef
    • Fracture Resistance of Heat-Treated Nickel-Titanium Rotary Files After Usage and Autoclave Sterilization: An In Vitro Study
      Rashid El Abed, Aisha Alshehhi, Yoo Jung Kang, Dana Al Raeesi, Amar H. Khamis, Mohamed Jamal, Hyeon-Cheol Kim
      Journal of Endodontics.2022; 48(11): 1428.     CrossRef
    • Effect of Autoclaving Cycles on the Cyclic Fatigue Resistance of Race and Race Evo Nickel-Titanium Endodontic Rotary Files: An In Vitro Study
      Rahaf A. Almohareb, Reem Barakat, Aroob Albakri, Manal Altamimi
      Metals.2021; 11(12): 1947.     CrossRef
    • Effect of number of uses and sterilization on the instrumented area and resistance of reciprocating instruments
      Victor de Ornelas Peraça, Samantha Rodrigues Xavier, Fabio de Almeida Gomes, Luciane Geanini Pena dos Santos, Erick Miranda Souza, Fernanda Geraldo Pappen
      Restorative Dentistry & Endodontics.2021;[Epub]     CrossRef
    • Influence of sterilization procedures on the physical and mechanical properties of rotating endodontic instruments: a systematic review and network meta-analysis
      Mario Dioguardi, Claudia Arena, Diego Sovereto, Riccardo Aiuto, Luigi Laino, Gaetano Illuzzi, Enrica Laneve, Bruna Raddato, Vito Carlo Alberto Caponio, Antonio Dioguardi, Khrystyna Zhurakivska, Giuseppe Troiano, Lorenzo Lo Muzio
      Frontiers in Bioscience-Landmark.2021;[Epub]     CrossRef
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    • 10 Download
    • 12 Crossref
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