Microtensile bond strength of self-etching and self-adhesive resin cements to dentin and indirect composite resin

Jae-Gu Park; Young-Gon Cho; Il-Sin Kim

doi:10.5395/JKACD.2010.35.2.106

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Basic Research Microtensile bond strength of self-etching and self-adhesive resin cements to dentin and indirect composite resin: Jae-Gu Park¹, Young-Gon Cho¹, Il-Sin Kim²; 2010;35(2):-115.
DOI: https://doi.org/10.5395/JKACD.2010.35.2.106
Published online: March 31, 2010

¹Department of Conservative Dentistry, College of Dentistry, Chosun University, Gwangju, Korea.

²Department of Dentistry, Graduated School of Chonnam National University, Gwangju, Korea.

Corresponding Author: Young-Gon Cho. Department of Conservative Dentistry, Chosun University, 421 Seosuk-dong, Dong-gu, Gwangju, 501-825, Korea. Tel: 82-62-220-3840, Fax: 82-62-232-9064, ygcho@chosun.ac.kr

• Received: February 1, 2010 • Revised: February 23, 2010 • Accepted: March 11, 2010

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Abstract
REFERENCES

Abstract

The purpose of this study was to evaluate the microtensile bond strength (µTBS), failure modes and bonding interfaces of self-etching and three self-adhesive resin cements to dentin and indirect composite resin.

Cylindrical composite blocks (Tescera, Bisco Inc.) were luted with resin cements (PA: Panavia F 2.0, Kuraray Medical Inc., RE: RelyX Unicem Clicker, 3M ESPE., MA: Maxem, Kerr Co., BI: BisCem, Bisco Inc.) on the prepared occlusal dentin surfaces of 20 extracted molars. After storage in distilled water for 24 h, 1.0 mm × 1.0 mm composite-dentin beams were prepared. µTBS was tested at a cross-head speed of 0.5 mm/min. Data were analyzed with one-way ANOVA and Tukey's HSD test. Dentin sides of all fractured specimens and interfaces of resin cements-dentin or resin cements-composite were examined at FE-SEM (Field Emission-Scanning Electron Microscope).

In conclusion, PA and RE showed higher bond strength and closer adaptation than MA and BI when indirect composite blocks were luted to dentin using a self-etching and three self-adhesive resin cements.
Keywords: Microtensile bond strength; Self-etching resin cement; Self-adhesive resin cement; Dentin; Indirect composite resin

Figure 1

SEM micrograph of dentin side showing a representative cohesive failure within Panavia F 2.0 (× 130).

Figure 2

SEM micrograph showing remnant fractured filler (F) and cement (C) on the surface of fractured Panavia F 2.0 (× 5,000).

Figure 3

SEM micrograph of dentin side showing a representative mixed failure with a thin layer of RelyX Unicem Clicker on the dentin surface (× 130).

Figure 4

SEM micrograph of dentin side showing a representative adhesive failure of Maxcem along dentin surface (× 130).

Figure 5

SEM micrograph showing remnant a few small sized filler (F) and cement (C) on the dentin surface and fractured Maxem (× 5,000).

Figure 6

SEM micrograph of dentin side showing a representative adhesive failure of BisCem along dentin surface (× 130).

Figure 7

SEM micrograph showing gap (G), about 5 µm wide, between the composite resin (R)-Panavia F 2.0 (P), and close adaptation with numerous short and long resin tags between the Panavia F 2.0-dentin (D) (× 600).

Figure 8

SEM micrograph showing wide gap (G), about 70 µm wide, between the composite resin (R)-RelyX Unicem Clicker (RU), and close adaptation with a few short resin tags between RelyX Unicem Clicker-dentin (D) (× 600).

Figure 9

SEM micrograph showing wide gap (G), about 60 µm wide, between the composite resin (R)-Maxcem (M), and discontinuous 1-2 µm wide gaps(g) between Maxem-dentin (D) (× 600).

Figure 10

SEM micrograph showing gap (G), about 15 µm wide, and a few short resin tags between BisCem (B)-dentin (D) (× 600).

Table 1

Resin cements

Table 2

Composition of resin cements

HEMA: 2-hydroxyethly methacrylate, 10-MDP:10-methacryloyloxydecyl dihydrogen phosphate, 5-NMSA: N-methacryloyl 5-aminosalicylic acid, GPDM: glycerol dimethacrylate dihydrogen phosphate; CQ: camphorquinone.

Table 3

Mean microtensile bond strength (MPa) to dentin and failure mode

PA; Panavia F 2.0, RE; RelyX Unicem Clicker, MA; Maxem, BI; BisCem

Superscripts of the same letter indicate values of statistically no significant difference by one-way ANOVA and Tukey's HSD test.

REFERENCES

1. Hikita K, Van Meerbeek B, De Munck J, Ikeda T, Van Landuyt K, Maida T, Lambrechts P, Peumans M. Bonding effectiveness of adhesive luting agents to enamel and dentin. Dent Mater. 2007;23: 71-80.Article PubMed
2. Lutz F, Krejci I, Barbaknow F. Quality and durability of marginal adaptation in bonded composite restorations. Dent Mater. 1991;7: 107-113.Article PubMed
3. El Zohairy AA, De Gee AJ, Mohsen MM, Feilzer AJ. Microtensile bond strength testing of luting cements to prefabricated CAD/CAM ceramic and composite blocks. Dent Mater. 2003;19: 575-583.Article PubMed
4. Song MH, Park SJ, Cho HG, Hwang YC, Oh WM, Hwang IN. Influence of adhesive application on shear bond strength of the resin cement to indirect resin composite. J Korean Acad Conserv Dent. 2008;33: 419-426.Article
5. Duarte S, Botta AC, Meire M, Saden A. Microtensile bond strength and scanning electron microscopic evaluation of self-adhesive and self-etch resin cements to intact and etched enamel. J Prosthet Dent. 2008;100: 203-210.PubMed
6. Mak YF, Lai SCN, Cheung GSP, Chan AWK, Tay FR, Pashley DH. Micro-tensile bond testing of resin cements to dentin and indirect resin composite. Dent Mater. 2002;18: 609-621.PubMed
7. Goracci C, Cury AH, Cantoro A, Papacchini F, Tay FR, Ferrari M. Microtensile bond strength and interfacial properties of self-etching and self-adhesive resin cements used to lute composite onlays under different seating forces. J Adhes Dent. 2006;8: 327-335.PubMed
8. Hiraishi N, Yiu CKY, King NM, Tay FR. Effect of pulpal pressure on the microtensile bond strength of luting resin cements to human dentin. Dent Mater. 2009;25: 58-66.Article PubMed
9. Jayasooriya PR, Perira PN, Nikaido T, Tagami J. Efficacy of a resin coating on bond strengths of resin cement to dentin. J Esthet Restor Dent. 2003;15: 105-113.Article PubMed
10. De Munck J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto-adhesive luting material to enamel and dentin. Dent Mater. 2004;20: 963-971.PubMed
11. Al-Assaf K, Chakmakchi M, Palaghias G, Karanika-Kouma A, Eliades G. Interfacial characteristics of adhesive luting resins and composites with dentine. Dent Mater. 2007;23: 829-839.Article PubMed
12. Yang B, Ludwig K, Adelung R, Kern M. Micro-tensile bond strength of three luting resins to human regional dentin. Dent Mater. 2006;22: 45-56.Article PubMed
13. Della Bona A, van Noort R. Shear vs tensile bond strength of resin composite bonded to ceramic. J Dent Res. 1995;74: 1591-1596.Article PubMed PDF
14. Chersoni S, Suppa P, Grandini S, Goracci G, Monticelli F, Yiu C. In vivo and vitro permeability of one-step self-etch adhesives. J Dent Res. 2004;83: 459-464.Article PubMed PDF
15. Han SH, Cho YG. Effect of a desensitizer on dentinal bond strength in cementation of composite resin inlay. J Korean Acad Conserv Dent. 2009;34: 223-231.Article
16. Kim DS, Park SH, Choi KW, Choi KK. The effect of bonding resin on bond strength of dual-cure resin cements. J Korean Acad Conserv Dent. 2007;32: 426-436.Article
17. Abo-Hamar SE, Hiller KA, Jung H, Federlin M, Friedl KH, Schmalz G. Bond strength of a new universal self-adhesive resin luting cement to dentin and enamel. Clin Oral Investig. 2005;9: 161-167.Article PubMed PDF
18. Monticelli F, Osorio R, Mazzitelli C, Ferrari M, Toledano M. Limited decalcification/diffusion of self-adhesive cements into dentin. J Dent Res. 2008;87: 974-976.Article PubMed PDF
19. Mazzitelli C, Monticelli F, Osorio R, Casucci A, Toledano M, Ferrari M. Effect of simulated pulpal pressure on self-adhesive cements bonding to dentin. Dent Mater. 2008;24: 1156-1163.Article PubMed
20. Moszner N, Salz U, Zimmermann J. Chemical aspects of self-etching enamel-dentin adhesives: a systematic review. Dent Mater. 2005;21: 895-910.Article PubMed
21. Shortall AC, Baylis RL, Wilson HJ. Composite inaly/luting resin bond strength-surface tratment effects. J Dent. 1996;24: 129-135.PubMed

Tables & Figures

Figure 1

SEM micrograph of dentin side showing a representative cohesive failure within Panavia F 2.0 (× 130).

Figure 2

SEM micrograph showing remnant fractured filler (F) and cement (C) on the surface of fractured Panavia F 2.0 (× 5,000).

Figure 3

SEM micrograph of dentin side showing a representative mixed failure with a thin layer of RelyX Unicem Clicker on the dentin surface (× 130).

Figure 4

SEM micrograph of dentin side showing a representative adhesive failure of Maxcem along dentin surface (× 130).

Figure 5

SEM micrograph showing remnant a few small sized filler (F) and cement (C) on the dentin surface and fractured Maxem (× 5,000).

Figure 6

SEM micrograph of dentin side showing a representative adhesive failure of BisCem along dentin surface (× 130).

Figure 7

Figure 8

Figure 9

SEM micrograph showing wide gap (G), about 60 µm wide, between the composite resin (R)-Maxcem (M), and discontinuous 1-2 µm wide gaps(g) between Maxem-dentin (D) (× 600).

Figure 10

SEM micrograph showing gap (G), about 15 µm wide, and a few short resin tags between BisCem (B)-dentin (D) (× 600).

Table 1

Resin cements

Table 2

Composition of resin cements

Table 3

Mean microtensile bond strength (MPa) to dentin and failure mode

PA; Panavia F 2.0, RE; RelyX Unicem Clicker, MA; Maxem, BI; BisCem

Superscripts of the same letter indicate values of statistically no significant difference by one-way ANOVA and Tukey's HSD test.

REFERENCES

1. Hikita K, Van Meerbeek B, De Munck J, Ikeda T, Van Landuyt K, Maida T, Lambrechts P, Peumans M. Bonding effectiveness of adhesive luting agents to enamel and dentin. Dent Mater. 2007;23: 71-80.Article PubMed
2. Lutz F, Krejci I, Barbaknow F. Quality and durability of marginal adaptation in bonded composite restorations. Dent Mater. 1991;7: 107-113.Article PubMed
3. El Zohairy AA, De Gee AJ, Mohsen MM, Feilzer AJ. Microtensile bond strength testing of luting cements to prefabricated CAD/CAM ceramic and composite blocks. Dent Mater. 2003;19: 575-583.Article PubMed
4. Song MH, Park SJ, Cho HG, Hwang YC, Oh WM, Hwang IN. Influence of adhesive application on shear bond strength of the resin cement to indirect resin composite. J Korean Acad Conserv Dent. 2008;33: 419-426.Article
5. Duarte S, Botta AC, Meire M, Saden A. Microtensile bond strength and scanning electron microscopic evaluation of self-adhesive and self-etch resin cements to intact and etched enamel. J Prosthet Dent. 2008;100: 203-210.PubMed
6. Mak YF, Lai SCN, Cheung GSP, Chan AWK, Tay FR, Pashley DH. Micro-tensile bond testing of resin cements to dentin and indirect resin composite. Dent Mater. 2002;18: 609-621.PubMed
7. Goracci C, Cury AH, Cantoro A, Papacchini F, Tay FR, Ferrari M. Microtensile bond strength and interfacial properties of self-etching and self-adhesive resin cements used to lute composite onlays under different seating forces. J Adhes Dent. 2006;8: 327-335.PubMed
8. Hiraishi N, Yiu CKY, King NM, Tay FR. Effect of pulpal pressure on the microtensile bond strength of luting resin cements to human dentin. Dent Mater. 2009;25: 58-66.Article PubMed
9. Jayasooriya PR, Perira PN, Nikaido T, Tagami J. Efficacy of a resin coating on bond strengths of resin cement to dentin. J Esthet Restor Dent. 2003;15: 105-113.Article PubMed
10. De Munck J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto-adhesive luting material to enamel and dentin. Dent Mater. 2004;20: 963-971.PubMed
11. Al-Assaf K, Chakmakchi M, Palaghias G, Karanika-Kouma A, Eliades G. Interfacial characteristics of adhesive luting resins and composites with dentine. Dent Mater. 2007;23: 829-839.Article PubMed
12. Yang B, Ludwig K, Adelung R, Kern M. Micro-tensile bond strength of three luting resins to human regional dentin. Dent Mater. 2006;22: 45-56.Article PubMed
13. Della Bona A, van Noort R. Shear vs tensile bond strength of resin composite bonded to ceramic. J Dent Res. 1995;74: 1591-1596.Article PubMed PDF
14. Chersoni S, Suppa P, Grandini S, Goracci G, Monticelli F, Yiu C. In vivo and vitro permeability of one-step self-etch adhesives. J Dent Res. 2004;83: 459-464.Article PubMed PDF
15. Han SH, Cho YG. Effect of a desensitizer on dentinal bond strength in cementation of composite resin inlay. J Korean Acad Conserv Dent. 2009;34: 223-231.Article
16. Kim DS, Park SH, Choi KW, Choi KK. The effect of bonding resin on bond strength of dual-cure resin cements. J Korean Acad Conserv Dent. 2007;32: 426-436.Article
17. Abo-Hamar SE, Hiller KA, Jung H, Federlin M, Friedl KH, Schmalz G. Bond strength of a new universal self-adhesive resin luting cement to dentin and enamel. Clin Oral Investig. 2005;9: 161-167.Article PubMed PDF
18. Monticelli F, Osorio R, Mazzitelli C, Ferrari M, Toledano M. Limited decalcification/diffusion of self-adhesive cements into dentin. J Dent Res. 2008;87: 974-976.Article PubMed PDF
19. Mazzitelli C, Monticelli F, Osorio R, Casucci A, Toledano M, Ferrari M. Effect of simulated pulpal pressure on self-adhesive cements bonding to dentin. Dent Mater. 2008;24: 1156-1163.Article PubMed
20. Moszner N, Salz U, Zimmermann J. Chemical aspects of self-etching enamel-dentin adhesives: a systematic review. Dent Mater. 2005;21: 895-910.Article PubMed
21. Shortall AC, Baylis RL, Wilson HJ. Composite inaly/luting resin bond strength-surface tratment effects. J Dent. 1996;24: 129-135.PubMed

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Microtensile bond strength of self-etching and self-adhesive resin cements to dentin and indirect composite resin

J Korean Acad Conserv Dent. 2010;35(2):106-115. Published online March 31, 2010

DOI: https://doi.org/10.5395/JKACD.2010.35.2.106

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Figure

Microtensile bond strength of self-etching and self-adhesive resin cements to dentin and indirect composite resin

Figure 1 SEM micrograph of dentin side showing a representative cohesive failure within Panavia F 2.0 (× 130).

Figure 2 SEM micrograph showing remnant fractured filler (F) and cement (C) on the surface of fractured Panavia F 2.0 (× 5,000).

Figure 3 SEM micrograph of dentin side showing a representative mixed failure with a thin layer of RelyX Unicem Clicker on the dentin surface (× 130).

Figure 4 SEM micrograph of dentin side showing a representative adhesive failure of Maxcem along dentin surface (× 130).

Figure 5 SEM micrograph showing remnant a few small sized filler (F) and cement (C) on the dentin surface and fractured Maxem (× 5,000).

Figure 6 SEM micrograph of dentin side showing a representative adhesive failure of BisCem along dentin surface (× 130).

Figure 7 SEM micrograph showing gap (G), about 5 µm wide, between the composite resin (R)-Panavia F 2.0 (P), and close adaptation with numerous short and long resin tags between the Panavia F 2.0-dentin (D) (× 600).

Figure 8 SEM micrograph showing wide gap (G), about 70 µm wide, between the composite resin (R)-RelyX Unicem Clicker (RU), and close adaptation with a few short resin tags between RelyX Unicem Clicker-dentin (D) (× 600).

Figure 9 SEM micrograph showing wide gap (G), about 60 µm wide, between the composite resin (R)-Maxcem (M), and discontinuous 1-2 µm wide gaps(g) between Maxem-dentin (D) (× 600).

Figure 10 SEM micrograph showing gap (G), about 15 µm wide, and a few short resin tags between BisCem (B)-dentin (D) (× 600).

Figure 1

Figure 2

Figure 3

Figure 4

Figure 5

Figure 6

Figure 7

Figure 8

Figure 9

Figure 10

Microtensile bond strength of self-etching and self-adhesive resin cements to dentin and indirect composite resin

Table 1

Resin cements

Table 2

Composition of resin cements

Table 3

Mean microtensile bond strength (MPa) to dentin and failure mode

PA; Panavia F 2.0, RE; RelyX Unicem Clicker, MA; Maxem, BI; BisCem

Superscripts of the same letter indicate values of statistically no significant difference by one-way ANOVA and Tukey's HSD test.

Table 1 Resin cements

Table 2 Composition of resin cements

Table 3 Mean microtensile bond strength (MPa) to dentin and failure mode

PA; Panavia F 2.0, RE; RelyX Unicem Clicker, MA; Maxem, BI; BisCem

Superscripts of the same letter indicate values of statistically no significant difference by one-way ANOVA and Tukey's HSD test.