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Original Article The effect of hybrid layer thickness on microtensile bond strength of three-step and self-etching dentin adhesive systems
Hye-Jung Lee, Jeong-Kil Park, Bock Hur
2003;28(6):-497.
DOI: https://doi.org/10.5395/JKACD.2003.28.6.491
Published online: November 30, 2003

Department of Conservative dentistry, College of Dentistry, Pusan National University, Korea.

Corresponding author (momosori@freechal.com)

Copyright © 2003 Korean Academy of Conservative Dentistry

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  • The purpose of this study was to evaluate the correlation between hybrid layer thickness and bond strength using confocal laser scanning microscope and microtensile bond strength test of two adhesive systems.
    The dentin surface of human molars, sectioned to remove the enamel from the occlusal surface. Either Scotchbond Multi-Purpose(3M Dental Product, St. Paul, MN, U.S.A) or Clearfil SE Bond(Kuraray, Osaka, Japan) was bonded to the surface, and covered with resin-composite. The resin-bonded teeth were serially sliced perpendicular to the adhesive interface to measure the hybrid layer thickness by confocal laser scanning microscope. The specimen were trimmed to give a bonded cross-sectional surface area of 1mm2, then the micro-tensile bone test was performed at a crosshead speed of 1.0 mm/min. All fractured surfaces were also observed by stereomicroscope.
    There was no significant differences in bond strengths the materials(p>0.05). However, the hybrid layers of three-step dentin adhesive system, SM, had significantly thicker than self-etching adhesive system, CS(p<0.05). Pearson's correlation coefficient showed no correlation between hybrid layer thickness and bond strengths(p>0.05). Bond strengths of dentin adhesive systems were not dependent on the thickness of hybrid layer.
  • Keywords: Hybrid layer thickness; Microtensile bond strength; Confocal laser scanning microscope
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Fig. 1
Scotchbond Multi-Purpose (3M)
A; Adhesive layer(rhodamine)
B; Primer layer(fluorescene)
C; Adhesive layer+Primer layer
jkacd-28-491-g001.jpg
Fig. 2
Clearfil SE Bond (Kuraray)
A; Adhesive layer(rhodamine)
B; Primer layer(fluorescene)
C; Adhesive layer+Primer layer
jkacd-28-491-g002.jpg
Table 1
Dentin bonding system used in this study
jkacd-28-491-i001.jpg
Table 2
Thickness of hybrid layer(THL) and microtensile bond strength(MTBS)
jkacd-28-491-i002.jpg
Table 3
Failure mode

type A : adhesive failure between bonding resin and dentin

type B : mixed failure (above 50% adhesive failure)

type C : mixed failure (below 50% adhesive failure)

type D : cohesive failure in resin

type E : cohesive failure in dentin

jkacd-28-491-i003.jpg

Tables & Figures

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    • Techniques for the restorative management of localized and generalized tooth wear
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      Dental Update.2023; 50(10): 842.     CrossRef

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      The effect of hybrid layer thickness on microtensile bond strength of three-step and self-etching dentin adhesive systems
      J Korean Acad Conserv Dent. 2003;28(6):491-497.   Published online November 30, 2003
      DOI: https://doi.org/10.5395/JKACD.2003.28.6.491
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    The effect of hybrid layer thickness on microtensile bond strength of three-step and self-etching dentin adhesive systems
    Image Image
    Fig. 1 Scotchbond Multi-Purpose (3M) A; Adhesive layer(rhodamine) B; Primer layer(fluorescene) C; Adhesive layer+Primer layer
    Fig. 2 Clearfil SE Bond (Kuraray) A; Adhesive layer(rhodamine) B; Primer layer(fluorescene) C; Adhesive layer+Primer layer

    Fig. 1

    Fig. 2

    The effect of hybrid layer thickness on microtensile bond strength of three-step and self-etching dentin adhesive systems

    Dentin bonding system used in this study

    Thickness of hybrid layer(THL) and microtensile bond strength(MTBS)

    Failure mode

    type A : adhesive failure between bonding resin and dentin

    type B : mixed failure (above 50% adhesive failure)

    type C : mixed failure (below 50% adhesive failure)

    type D : cohesive failure in resin

    type E : cohesive failure in dentin
    Table 1 Dentin bonding system used in this study

    Table 2 Thickness of hybrid layer(THL) and microtensile bond strength(MTBS)

    Table 3 Failure mode

    type A : adhesive failure between bonding resin and dentin

    type B : mixed failure (above 50% adhesive failure)

    type C : mixed failure (below 50% adhesive failure)

    type D : cohesive failure in resin

    type E : cohesive failure in dentin

    Table 1

    Table 2

    Table 3

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